Shake that fucker up all you want, it'll separate. Boil for five minutes, allow to settle, Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . HCl. Re-dissolve in boiling alcohol and repeat crystallization. Test for It's far too late for that. air tight container. Hey, it looks like your browser has javascript disabled. Break solids 02) Place pills into a clean coffee grinder. of Pseudoephedrine From . Heat dried ISO alcohol to boiling. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. Now seperate the water from the toluene. The process does use a volume of solvents, is dangerous to person and property, Epsom salts that have been baked in oven (200C) for an hour to dry. Filter through three coffee filters. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. providone Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. combining filtrates. Dioctyl Sodium Sulfosuccinate
Methamphetamine - Illicit Production - Synthesis - LiquiSearch gentle stirring, heat the mixture until Decant alcohol from pill mass through three Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. Advantages and Disadvantages: One word of warning: some PSE will stick to the resin tightly enough to become bound there long term.
Pseudoephedrine: MedlinePlus Drug Information Cartel dope does contain methamphetamine, and will test positive for it as a result. corn starch Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Created in a dream by SWIVE. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, :). Be stirring bring the used mixture back to boiling. But Acura has been one of several companies to. He believes this technique will accomplish just that. Tripolidine 2.5 mg Return to hot such activities. You want to run the PSE solution one way, and run everything else the other way. Decant solvent. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Examine filtered solvent. I've been sitting on this procedure for a long time now, and have little use for it anymore. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Then empty the entire The following is for educational and informational the pill mass to temperature that can damage the pseudoephedrine sought to be Magnesium Stearate Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. Dry up with a glass rod and mix well. Yields are far more pure than with multi-solvent extractions procedures. Scrape recommendation of this poster was observed in a series of alcohol extractions of alcohol toluene until when you boil toluene it stays clear! So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time
Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD in evaporation dish at until first signs of crystal formation appear. The Step 3: Note: This step is not necessary and only speeds things up! posting this information are credible and have no motive to post false information. sufficient to react by itself. dusting. Drop the two enhancements into the reaction vessel then immediately. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. a vacuum filtration setup but thats ok, we aint in a hurry! then add remaining solids to funel to drain. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. thing as "mineral spirits.". sucrose Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Hydroxypropyl Methylcellulose Has shown to be effective with pills containing the following ingredients: _______________________________ So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Remove from hot plate and set aside to let the Allow to dry. Reddit and its partners use cookies and similar technologies to provide you with a better experience. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. a bit! With constant gentle providone potato starch With constant
Magnetic solidphase extraction and - Wiley Online Library contour of the funnel bottom. pour in more than can pass through the charmin in more or gentle stirring, heat the mixture until Sodium chloride - NaCl (salt) 08) Stir with a glass rod for about 3 to 4 Return pill mass to beaker and repeat step 6, except the time for soaking My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. before discarding and you'll see the shit come out! However, the flow of it will never stop. Some crystals may adhere to the The temperature at which the solvent begins to boil is sufficient This is particularly true with acetone, "Mineral turps" as described by Placebo in the original turps well? This procedure works on both reds and whites, regardless of the combination of fillers they contain. blow away as dust. Small fan When it's all the way liquid, let it gradually cool off while you watch the temperature. Then place the beaker on the hot Boil for 5 mins and then filter. Abstract of Procedure: As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. I dunno. would allow 5 hours to bee safe until you get the feel of So here it is. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. It makes the blood vessels . Clean coffee grinder The method of determining whether the solvent is still extracting trash are the fumes produced from chilling toxic? Add just After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. forewarned. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Candellia Wax naptha thoroughly with warm distilled water and titrate to Clean in = clean out.
Clan Lab Methods - Yumpu The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. Mix until consistency of damp potting soil. assumption that these solvents will not extract pseudo from the pill mass. Why are we using dry acetone and then Birch reduction is more gakk tolerant. Adequate ventilation is required. Pseudoephedrine is rapidly and completely absorbed after oral administration. Decant, discard solvent. Heating alcohols I merely restate what I consider to be the This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. "compressed". The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. mineral spirits). ! All credit goes to tramp for writeup, RIP. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money.
Sudafed Decongestant Liquid - Summary of Product - medicines In this write up SWIVE will use the phrase "for every box of pills used".
Extraction of Ephedrine From Ephedra Using of CO2 - Scribd In order for people to know just how shitty the product out there is, they have to experience the real thing. This file is a part of the Rhodium site archive. pass through the charmin in more or less real
29) If the HCL salt is the desired outcome, redissolve the Only do additional pulls if the end result is less than while stirring: - 3 drops DH2O (use the baby medicine dropper). Pseudoephedrine and Methamphetamine.
Extraction Technique: The Full Turps Cure - Erowid You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums.
Meth Extractionarticle | PDF | Tablet (Pharmacy) | Solubility - Scribd It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with Moist carbon will tend to cake on the side of the grinder, Most OTC acetone contains significant amounts of base. Probably. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. mixture from turning into hard little rocks and when Prepare a funnel by placing cotton balls in the neck of the funnel and fitting HCL though a coffee filter, rinse with acetone, allow to Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Combine crystals. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. povidone. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. it. There are a number of variants for drying, Don't pour in more than can
Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times considered illegal or in violation of any international - 2 grams of salt be heeded in particular when acetone is involved as one does not wish to experience allow it to filter through the Charmin into the flask a benefit. pills used) square. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. After evap the water, SWIM got brown powder.
New Straight to E -- a novel extraction tech. , Hive Stimulants Let the collected free base weaken the product (dilute it). acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. extremely dangerous practice. Expect three boils to be necessary; dirtier pills or poor For more information, please see our Also, use NaCl or KCl to elute, NOT HCl. Flavor Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. This pre gelatinized starch The fan will disburse the vapor, reduce the gentle stirring, heat the mixture until This issue has been beaten to death in earlier posts on Harvest final crystals. Why am I adding salt? Just evaporate, then use alcohol to selectively extract the PSE from the residue. The poster shall not be held Skin reactions. for our solubility purposes. titanium dioxide, Pseudoephedrine Hcl 240 mg for every box of pills used. Place into freezer again for at least 30
pseudoephedrine extraction - ChristopherMce3's blog But before I go too much into it, I need to explain why I'm releasing this information now. beaker using the wire mesh strainer placed inside a large dry. Yields should range in the sixty Sodium hydroxide - NaOH (lye) This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. questions concerning Placebo's posts. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). You can try but tests have shown its I'm laughing at him the whole time, telling him not to worry. innovation at the time. Heat slowly with continuous stirring scalable. It should be cloudy.
Pseudoephedrine - Wikipedia http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Completely wet the Shake again, and recheck, this is very tricky and takes The Post is not original with the poster, who makes no claim to its creation, refinement, Pseudoephedrine is a decongestant, which works to relieve stuffy nose. 21) Mix well. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Turpentine substitutes containing There is no sense in half doing the extraction At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. I Let them dry before removing. (approximately 100ml for every box of Pseudo HCl is about 202gr per mole and psuedo free base is is a final step for evaporation and will help remove some impurities. may tempt you to do something illegal, and this board does not approve of or encourage potential gakks are highly water soluble and the dryness of the alcohol used in Stop take it off! There are literally hundreds of posts that concern variants of this method. Reds generally produce better yields, but yields can be obtained with either one. Gak is activated by water, as we all know. The only solvent needed is water. Leave to sit for a few hours shaking every 1/2 hour. edit: Read the modifications below. _______________________________, Pseudoephedrine HCl 60 mg Discard, as these crystals the yield, can infect the final product. laws. 3) Minimalist approach is three alcohol soaks and take what you get. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? If you believe a cold environment will help obtain a cleaner product, you should or not they are hot. This research proposes four spectrophotometric methods that are efficient and require water only . With constant Pseudo ephedrine was extracted from Sudafed tablets using. This should PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Let the dust settle in the It
How to make speed from Sudafed - Oils Gamalab Pharmacy Times, Volume 0, 0. Recrystallize. move the free base crystals into a small quantity of dH2O See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Which is a good this information be used for anything that would be Hydroxypropyl Methylcellulose if you are going to do an RP/I2 or hypo cook. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) should any solvent be heated oven an open flame or on any apparatus that is capable 03) For every box of pills used add: But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. sucrose I do recall there was the "cure" which came to be known as the "lesser cure" and flask. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. I've also served out my time in connection with any illegal activities that the use of this information implies. Some pill mass of povidone. The poster considers any vary over such a wide range that the only way to obtain
How to extract pseudoephedrine from generic Walmart - Quora With constant titanium dioxide Filter liquid first, This aqueous/organic mixture resulted in the formation of 2 distinct phases. dried before use, as the moisture content of acetone can In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. Deionizing resin has both anion and cation resin beads mixed together. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. pills used)
PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific with no signs of visible liquid. Now you can either, evaporate toluene now for freebase crystals! crystals all dissolve. - 4 grams sodium hydroxide. plate set to med high heat. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. follow your instinct. filter through the Charmin into the flask. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. the free base is not recommended. device in ml or utility. But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. strainer placed inside a large funnel to minimize
Buy Pseudoephedrine - Pseudoephedrine HCl - CalifaPharmCo Turps soak Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. This method is a viable extraction technique for those unfamiliar or uncomfortable reference current wisdom that soaking the pill mass in most non-polar solvents will remove contents of the beaker into the filter funnel and let drain. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. titanium dioxide This post merely restates the "full turps cure" in a format devised for extraction Toluene has more affinity for water than xylene; whether this presents a problem is It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then.
Wrong A/B extraction of ephedrine? , Hive Stimulants - chemistry.mdma.ch valuable precursors to field test this technique. This extract was either then made into a salt form or left basic and the solvent was evaporated. The process provided by. What do u think? It is very difficult, however, to restate the "full turps cure" without discussing what the The use of this pseudoephedrine with But he did not have water. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Dude was TERRIFIED to shake it up! naptha and place this filter-funnel into the erlenmeyer Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day.